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1 article(s) from Lant, Hannah M C

Comparison of the catalytic activity for the Suzuki–Miyaura reaction of (η⁵-Cp)Pd(IPr)Cl with (η³-cinnamyl)Pd(IPr)(Cl) and (η³-1-t-Bu-indenyl)Pd(IPr)(Cl)

Patrick R. Melvin,
Nilay Hazari,
Hannah M. C. Lant,
Ian L. Peczak and
Hemali P. Shah

Beilstein J. Org. Chem. 2015, 11, 2476–2486, doi:10.3762/bjoc.11.269

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Graphical Abstract

Figure 1: General depictions of allyl and related precatalysts that are highly active for the Suzuki–Miyaura ...

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Scheme 1: Synthesis of Cp.

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Figure 2: Comparison of catalytic performance of Cin, Cp and ^tBuInd for a series of Suzuki–Miyaura reactions ...

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Figure 3: Comparison of catalytic performance of Cin, Cp and ^tBuInd for a series of Suzuki–Miyaura reactions ...

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Scheme 2: Proposed mechanism for the activation of Cp to monoligated Pd(0).

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Scheme 3: Synthesis of Cp^Dim.

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Figure 4: ORTEP of Cp^Dim at 30% probability. Hydrogen atoms and isopropyl groups of IPr are omitted for clari...

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Scheme 4: Observation of Cp^Dim under modified catalytic conditions.

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Scheme 5: Cp^Dim is not an active precatalyst for a Suzuki–Miyaura reaction at room temperature.

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Scheme 6: Disproportionation of Cp^Dim with dvds.

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Scheme 7: a) Crossover experiment between Cp and (μ-allyl)(μ-Cl)Pd₂(IPr)₂. b) Crossover experiment expressed ...

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Published 08 Dec 2015

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Comparison of the catalytic activity for the Suzuki–Miyaura reaction of (η5-Cp)Pd(IPr)Cl with (η3-cinnamyl)Pd(IPr)(Cl) and (η3-1-t-Bu-indenyl)Pd(IPr)(Cl)

Comparison of the catalytic activity for the Suzuki–Miyaura reaction of (η⁵-Cp)Pd(IPr)Cl with (η³-cinnamyl)Pd(IPr)(Cl) and (η³-1-t-Bu-indenyl)Pd(IPr)(Cl)